1-Propene, 3-[2,3-bis(2-iodoethoxy)propoxy]- synthesis

2synthesis methods

Product Name:1-Propene, 3-[2,3-bis(2-iodoethoxy)propoxy]-
CAS Number:114719-16-3
Molecular formula:C10H18I2O3
Molecular Weight:440.06

Ethanol, 2,2'-[[1-[(2-propen-1-yloxy)methyl]-1,2-ethanediyl]bis(oxy)]bis-

107106-38-7
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1-Propene, 3-[2,3-bis(2-iodoethoxy)propoxy]-

114719-16-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 60 percent / pyridine / Ambient temperature
2: 80 percent / NaI, Na₂CO₃ / acetone / 24 h / Heating

References:

Bradshaw, Jerald S.;Krakowiak, Krzysztof E.;Bruening, Ronald L.;Tarbet, Bryon J.;Savage, Paul B.;Izatt, Reed M. [Journal of Organic Chemistry,1988,vol. 53,# 14,p. 3190 - 3195]

Ethanol,2,2'-[[1-[(2-propenyloxy)methyl]-1,2-ethanediyl]bis(oxy)]bis-,bis(4-methylbenzenesulfonate)

114719-15-2
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114719-16-3
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References