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ChemicalBook CAS DataBase List 1-SILA-3-CYCLOPENTENE 95%

1-SILA-3-CYCLOPENTENE 95% synthesis

4synthesis methods
872-46-8 Synthesis
1,1-Dichloro-1-silacyclo-3-pentene

872-46-8
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Yield:7049-25-4 62%

Reaction Conditions:

with lithium aluminium tetrahydride in dibutyl ether at -15 - 20;Schlenk technique;Inert atmosphere;

References:

Duerden, Amanda J.;Grubbs, G. S.;Guirgis, Gamil A.;Laane, Jaan;Marshall, Frank E.;McFadden, Thomas M. C.;Moon, Nicole;Ocola, Esther J. [Physical Chemistry Chemical Physics,2022,vol. 24,# 4,p. 2454 - 2464]

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