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ChemicalBook CAS DataBase List 10-Fluorodecanoic acid

10-Fluorodecanoic acid synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: Nonafluorobutanesulfonyl fluoride; N-ethyl-N,N-diisopropylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere
2: sodium hydroxide / methanol; water / 6 h / 40 °C / Inert atmosphere

References:

Zhao, Yizhou;Chen, Yifeng;Newhouse, Timothy R. [Angewandte Chemie - International Edition,2017,vol. 56,# 42,p. 13122 - 13125][Angew. Chem.,2017,vol. 129,# 42,p. 13302 - 13305,4]