(alphaS)-alpha-[[[Methyl[[2-(1-Methylethyl)-4-thiazolyl]Methyl]aMino]carbonyl]aMino]-4-Morpholinebutanoic acid Methyl ester synthesis
- Product Name:(alphaS)-alpha-[[[Methyl[[2-(1-Methylethyl)-4-thiazolyl]Methyl]aMino]carbonyl]aMino]-4-Morpholinebutanoic acid Methyl ester
- CAS Number:1004316-91-9
- Molecular formula:C18H30N4O4S
- Molecular Weight:398.52
154212-60-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 25 °C
1.2: 7 h / 25 °C
2.1: dichloromethane / 1 h / 25 °C
3.1: sodium cyanoborohydride / water; acetonitrile; chloroform / 12 h / 25 °C
References:
GILEAD SCIENCES, INC.;CULLEN, Aaron, J.;YU, Richard, Hung Chiu WO2013/116715, 2013, A1
![Butanoic acid, 4-amino-2-[[[methyl[[2-(1-methylethyl)-4-thiazolyl]methyl]amino]carbonyl]amino]-, methyl ester, (2S)-, 2,2,2-trifluoroacetate (1:1)](/CAS/20211123/GIF/1004316-90-8.gif)
