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2-Methoxy-5,5-dimethyl-1,3,2-dioxaphosphorinane 2-oxide synthesis

8synthesis methods
-

Yield:4090-55-5 35 % Spectr. ,1005-96-5 65 % Spectr.

Reaction Conditions:

with tert-butylhypochlorite at 20;Product distribution;

References:

Harger, Martin J.P [Tetrahedron Letters,2001,vol. 42,# 38,p. 6749 - 6752]