6-Methyl-5-(2-methylpropyl)pyridine-3-carboxylic Acid Hydrochloride synthesis

4synthesis methods

Product Name:6-Methyl-5-(2-methylpropyl)pyridine-3-carboxylic Acid Hydrochloride
CAS Number:1011476-26-8
Molecular formula:C11H16ClNO2
Molecular Weight:229.7

41667-95-2 Synthesis

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6-Methyl-5-(2-methylpropyl)pyridine-3-carboxylic Acid Hydrochloride

1011476-26-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: toluene / 3 h / 80 °C
2.1: iron(III)-acetylacetonate / 1-methyl-pyrrolidin-2-one; tetrahydrofuran / -78 - 0 °C
2.2: -70 - -20 °C
3.1: iron(III)-acetylacetonate / 1-methyl-pyrrolidin-2-one; tetrahydrofuran / -78 - 20 °C
4.1: hydrogenchloride / 1,4-dioxane / 3 h

References:

US2011/212998,2011,A1

3-Pyridinecarboxylic acid, 6-methyl-5-(2-methylpropyl)-, 1,1-dimethylethyl ester

1011476-29-1
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1011476-26-8
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References

1011476-27-9 Synthesis

5,6-Dichloro-nicotinic acid tert-butyl ester

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References

3-Pyridinecarboxylic acid, 5-chloro-6-methyl-, 1,1-dimethylethyl ester

1011476-28-0
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1011476-26-8
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References