(3aS,5R,6R,6aS)-6-((tert-butyldiMethylsilyl)oxy)-2,2-diMethyltetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde synthesis

7synthesis methods

Product Name:(3aS,5R,6R,6aS)-6-((tert-butyldiMethylsilyl)oxy)-2,2-diMethyltetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde
CAS Number:1018898-77-5
Molecular formula:C14H26O5Si
Molecular Weight:302.44

α-L-Xylofuranose, 3-O-[(1,1-dimethylethyl)dimethylsilyl]-1,2-O-(1-methylethylidene)-

379269-17-7
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(3aS,5R,6R,6aS)-6-((tert-butyldiMethylsilyl)oxy)-2,2-diMethyltetrahydrofuro[2,3-d][1,3]dioxole-5-carbaldehyde

1018898-77-5
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Yield:1018898-77-5 99%

Reaction Conditions:

with 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical;trichloroisocyanuric acid in dichloromethane at 0 - 20;Inert atmosphere;

References:

Goodwin, Nicole C.;Mabon, Ross;Harrison, Bryce A.;Shadoan, Melanie K.;Almstead, Zheng Y.;Xie, Yiling;Healy, Jason;Buhring, Lindsey M.;DaCosta, Christopher M.;Bardenhagen, Jennifer;Mseeh, Faika;Liu, Qingyun;Nouraldeen, Amr;Wilson, Alan G. E.;Kimball, S. David;Powell, David R.;Rawlins, David B. [Journal of Medicinal Chemistry,2009,vol. 52,# 20,p. 6201 - 6204] Location in patent:supporting information; experimental part

α-L-Xylofuranose, 1,2-O-(1-methylethylidene)-, 5-benzoate

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114861-22-2 Synthesis

114861-22-2
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α-L-Xylofuranose, 3-O-[(1,1-dimethylethyl)dimethylsilyl]-1,2-O-(1-methylethylidene)-, 5-benzoate

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1018898-77-5
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609-06-3 Synthesis

609-06-3
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