ETHYL 5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)FURAN-3-CARBOXYLATE synthesis
- Product Name:ETHYL 5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)FURAN-3-CARBOXYLATE
- CAS Number:1025719-08-7
- Molecular formula:C13H19BO5
- Molecular Weight:266.1
614-98-2
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Yield: 73%
Reaction Conditions:
with (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-di-tert-butyl-2,2'-bipyridine in tetrahydrofuran at 80; for 18 h;Inert atmosphere;
References:
Robbins, Daniel W.;Hartwig, John F. [Organic Letters,2012,vol. 14,# 16,p. 4266 - 4269] Location in patent:supporting information; experimental part
