Ethyl 4-amino-1-(methoxymethyl)-1H-imidazole-2-carboxylate synthesis

4synthesis methods

Product Name:Ethyl 4-amino-1-(methoxymethyl)-1H-imidazole-2-carboxylate
CAS Number:1026411-22-2
Molecular formula:C8H13N3O3
Molecular Weight:199.21

20075-26-7 Synthesis

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Ethyl 4-amino-1-(methoxymethyl)-1H-imidazole-2-carboxylate

1026411-22-2
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 70 percent / CH₂Cl₂ / 3 h / Ambient temperature
2: 46 percent / HNO₃, acetic anhydride / 2 h / Ambient temperature
3: 96 percent / NaH / 1 h
4: H₂ / Pd/C / tetrahydrofuran

References:

Zhao;Al-Said;Sternbach;Lown [Journal of Medicinal Chemistry,1997,vol. 40,# 2,p. 216 - 225]

1H-Imidazole-2-carboxylic acid, 1-(methoxymethyl)-4-nitro-, ethyl ester

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1026411-22-2
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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1026411-22-2
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References

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1026411-22-2
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References