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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Benzoic acid, 2-(chlorosulfonyl)-, ethyl ester (9CI)
103008-54-4

Benzoic acid, 2-(chlorosulfonyl)-, ethyl ester (9CI) synthesis

1synthesis methods
2-Sulfobenzoic anhydride

81-08-3
198 suppliers
$5.00/1g

Benzoic acid, 2-(chlorosulfonyl)-, ethyl ester (9CI)

103008-54-4
13 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: ammonia / methanol / 2 h
2: thionyl chloride / N,N-dimethyl-formamide / Inert atmosphere; Reflux

References:

Jelier, Benson J.;Tripet, Pascal F.;Pietrasiak, Ewa;Franzoni, Ivan;Jeschke, Gunnar;Togni, Antonio [Angewandte Chemie - International Edition,2018,vol. 57,# 42,p. 13784 - 13789][Angew. Chem.,2018,vol. 130,p. 13980 - 13985,6]