Carbamic acid, N-[(1S)-2-(3-methoxyphenyl)-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester synthesis

1synthesis methods

Product Name:Carbamic acid, N-[(1S)-2-(3-methoxyphenyl)-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester
CAS Number:1034153-28-0
Molecular formula:C15H21NO4
Molecular Weight:279.33

15761-38-3 Synthesis

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Carbamic acid, N-[(1S)-2-(3-methoxyphenyl)-1-methyl-2-oxoethyl]-, 1,1-dimethylethyl ester

1034153-28-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 1,1'-carbonyldiimidazole / dichloromethane / 16 h / 0 - 15 °C / Industrial scale
2.1: isopropylmagnesium chloride / tetrahydrofuran / 1.66 h / 10 - 15 °C / Industrial scale
2.2: 10 - 15 °C / Industrial scale

References:

WO2013/1294,2013,A1