Naphtho[1,2-b]thiophene-2-carboxylic acid, 4,5-dihydro-5,5-dimethyl- synthesis

1synthesis methods

Product Name:Naphtho[1,2-b]thiophene-2-carboxylic acid, 4,5-dihydro-5,5-dimethyl-
CAS Number:1038304-09-4
Molecular formula:C15H14O2S
Molecular Weight:258.34

2979-69-3 Synthesis

4,4-DIMETHYL-3,4-DIHYDRO-2H-NAPHTHALEN-1-ONE

2979-69-3
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Naphtho[1,2-b]thiophene-2-carboxylic acid, 4,5-dihydro-5,5-dimethyl-

1038304-09-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: trichlorophosphate
2: sodium ethanolate
3: sodium hydroxide / tetrahydrofuran; water

References:

Han, Qiang;Pabba, Praveen K.;Barbosa, Joseph;Mabon, Ross;Healy, Jason P.;Gardyan, Michael W.;Terranova, Kristen M.;Brommage, Robert;Thompson, Andrea Y.;Schmidt, James M.;Wilson, Alan G.E.;Xu, Xiaolian;Tarver, James E.;Carson, Kenneth G. [Bioorganic and Medicinal Chemistry Letters,2016,vol. 26,# 4,p. 1184 - 1187]