5 - fluoro - 2 - (4 - Methoxy phenyl) (acetylene) benzaldehyde synthesis
- Product Name:5 - fluoro - 2 - (4 - Methoxy phenyl) (acetylene) benzaldehyde
- CAS Number:1042369-35-6
- Molecular formula:C16H11FO2
- Molecular Weight:254.26
94569-84-3
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$16.00/5g
768-60-5
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$6.00/1g
1042369-35-6
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$30.00/250mg
Yield:1042369-35-6 94%
Reaction Conditions:
Stage #1: 2-bromo-5-fluorobenzaldehyde;4-methoxyphenylacetylenwith trans-bis(triphenylphosphine)palladium dichloride;triethylamine at 20; for 0.166667 h;Inert atmosphere;Sonogashira Cross-Coupling;
Stage #2: with copper(l) iodide at 50; for 3 h;Inert atmosphere;Sonogashira Cross-Coupling;
References:
Dell'Acqua, Monica;Pirovano, Valentina;Peroni, Stefano;Tseberlidis, Giorgio;Nava, Donatella;Rossi, Elisabetta;Abbiati, Giorgio [European Journal of Organic Chemistry,2017,vol. 2017,# 11,p. 1425 - 1433] Location in patent:supporting information
877264-44-3
66 suppliers
$96.00/250mg
768-60-5
215 suppliers
$6.00/1g
1042369-35-6
29 suppliers
$30.00/250mg