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Benzoic acid, 3-bromo-4,5-dimethoxy-2-methyl-, methyl ester synthesis

1synthesis methods
Benzoic acid, 4,5-dimethoxy-2-methyl-, methyl ester

50525-09-2
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Benzoic acid, 3-bromo-4,5-dimethoxy-2-methyl-, methyl ester

1042722-40-6
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Yield:1042722-40-6 92%

Reaction Conditions:

with bromine in chloroform at 0; for 4.5 h;

References:

Kim, Joa Kyum;Kim, Young Ha;Nam, Ho Tae;Kim, Bum Tae;Heo, Jung-Nyoung [Organic Letters,2008,vol. 10,# 16,p. 3543 - 3546] Location in patent:supporting information; experimental part