Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 5-Benzyl-10-oxo-10,11-dihydro-5H-dibenz[b,f]azepine

5-Benzyl-10-oxo-10,11-dihydro-5H-dibenz[b,f]azepine synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 88 percent / NaOtBu / Pd(OAc)2; rac-BINAP / toluene
2: 97 percent / NaH / dimethylformamide
3: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C

References:

Lohse, Olivier;Beutler, Ulrich;Fünfschilling, Peter;Furet, Pascal;France, Julien;Kaufmann, Daniel;Penn, Gerhard;Zaugg, Werner [Tetrahedron Letters,2001,vol. 42,# 3,p. 385 - 389]

5-Benzyl-10-oxo-10,11-dihydro-5H-dibenz[b,f]azepine Related Search: