4',4''',4'''''-borylidynetris[2',3',5',6'-tetramethyl-[1,1'-Biphenyl]-4-carboxylic acid synthesis

1synthesis methods

Product Name:4',4''',4'''''-borylidynetris[2',3',5',6'-tetramethyl-[1,1'-Biphenyl]-4-carboxylic acid
CAS Number:1048667-04-4
Molecular formula:C51H51BO6
Molecular Weight:770.76

99768-12-4 Synthesis

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4',4''',4'''''-borylidynetris[2',3',5',6'-tetramethyl-[1,1'-Biphenyl]-4-carboxylic acid

1048667-04-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; ethanol; toluene
2: NaOH / tetrahydrofuran; methanol; sodium hydroxide

References:

Liu, Yan;Xuan, Weimin;Zhang, Hui;Cui, Yong [Inorganic Chemistry,2009,vol. 48,# 21,p. 10018 - 10023]