1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride synthesis
- Product Name:1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride
- CAS Number:104940-65-0
- Molecular formula:C13H12Cl2N4O4
- Molecular Weight:359.16
2140-11-6
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104940-65-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 83 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy free radical; iodosobenzene diacetate / acetonitrile; H2O / 4 h / 20 °C
2: SOCl2; DMF / CHCl3 / 5 h / Heating
References:
Middleton, Richard J.;Briddon, Stephen J.;Cordeaux, Yolande;Yates, Andrew S.;Dale, Clare L.;George, Michael W.;Baker, Julian G.;Hill, Stephen J.;Kellam, Barrie [Journal of Medicinal Chemistry,2007,vol. 50,# 4,p. 782 - 793]
28440-13-3
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104940-65-0
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58-63-9
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$5.00/25g
104940-65-0
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