Benzenepropanoic acid, 2-nitro-β-[(2-pyridinylcarbonyl)amino]- synthesis
- Product Name:Benzenepropanoic acid, 2-nitro-β-[(2-pyridinylcarbonyl)amino]-
- CAS Number:1056640-28-8
- Molecular formula:C15H13N3O5
- Molecular Weight:315.28
5678-48-8
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Yield:1056640-28-8 92%
Reaction Conditions:
Stage #1: 3-amino-3-(2-nitrophenyl)propionic acidwith 4-methyl-morpholine in N,N-dimethyl-formamide; for 0.0833333 h;Darkness;
Stage #2: 2-picolinoyl chloride hydrochloride in N,N-dimethyl-formamide at 80; for 3 h;Darkness;
References:
Kumbhar, Anupa A.;Franks, Andrew T.;Butcher, Raymond J.;Franz, Katherine J. [Chemical Communications,2013,vol. 49,# 24,p. 2460 - 2462] Location in patent:supporting information
