3-(3-NITRO-[1,2,4]TRIAZOL-1-YL)-PROPIONIC ACID METHYL ESTER synthesis
1synthesis methods
- Product Name:3-(3-NITRO-[1,2,4]TRIAZOL-1-YL)-PROPIONIC ACID METHYL ESTER
- CAS Number:105958-58-5
- Molecular formula:C6H8N4O4
- Molecular Weight:200.15
Yield:105958-58-5 80%
Reaction Conditions:
with N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide at 20; for 114 h;Inert atmosphere;regioselective reaction;Michael type addition;
References:
Boncel, Slawomir;Saletra, Kinga;Hefczyc, Barbara;Walczak, Krzysztof Z. [Beilstein Journal of Organic Chemistry,2011,vol. 7,p. 173 - 178] Location in patent:supporting information; experimental part