3-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1h-indole synthesis

3synthesis methods

Product Name:3-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1h-indole
CAS Number:1072812-35-1
Molecular formula:C15H20BNO2
Molecular Weight:257.14

83-34-1 Synthesis

83-34-1
493 suppliers
$12.00/10g

3-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1h-indole

1072812-35-1
13 suppliers
$167.00/250mg

1H-Indole, 3-Methyl-7-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-

1181825-29-5
13 suppliers
$499.70/5MG

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine / cyclohexane / 18 h / 60 °C / Schlenk technique; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Schlenk technique

References:

Kallepalli, Venkata A;Gore, Kristin A.;Shi, Feng;Sanchez, Luis;Chotana, Ghayoor A.;Miller, Susanne L.;Maleczka, Robert E.;Smith, Milton R. [Journal of Organic Chemistry,2015,vol. 80,# 16,p. 8341 - 8353]

83-34-1 Synthesis

83-34-1
493 suppliers
$12.00/10g

73183-34-3
578 suppliers
$6.00/5g

1072812-35-1
13 suppliers
$167.00/250mg

References

73183-34-3
578 suppliers
$6.00/5g

1072812-35-1
13 suppliers
$167.00/250mg

1181825-29-5
13 suppliers
$499.70/5MG

References