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tert-butyl 3-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate synthesis

2synthesis methods
-

Yield:1073493-92-1 97%

Reaction Conditions:

with (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;potassium acetate in dimethyl sulfoxide at 80; for 10 h;Inert atmosphere;Miyaura Borylation Reaction;

References:

Cao, Dennis;Juricek, Michal;Brown, Zachary J.;Sue, Andrew C.-H.;Liu, Zhichang;Lei, Juying;Blackburn, Anthea K.;Grunder, Sergio;Sarjeant, Amy A.;Coskun, Ali;Wang, Cheng;Farha, Omar K.;Hupp, Joseph T.;Stoddart, J. Fraser [Chemistry - A European Journal,2013,vol. 19,# 26,p. 8457 - 8465]