2-(5-chloro-1H-1,3-benzodiazol-2-yl)-6-methylphenol synthesis
1synthesis methods
- Product Name:2-(5-chloro-1H-1,3-benzodiazol-2-yl)-6-methylphenol
- CAS Number:1094405-95-4
- Molecular formula:C14H11ClN2O
- Molecular Weight:258.7
Yield:1094405-95-4 60%
Reaction Conditions:
Stage #1: 2-methoxy-3-methylbenzaldehydewith sodium hydrogensulfite in ethanol at 20;
Stage #2: 4-Chloro-1,2-phenylenediamine in ethanol;N,N-dimethyl-formamide; for 2 h;Reflux;
References:
Tavman, Aydin;Ikiz, Serkan;Bagcigil, A. Funda;?zgür, N. Yakut;Ak, Seyyal [Russian Journal of Inorganic Chemistry,2010,vol. 55,# 2,p. 215 - 222] Location in patent:experimental part