3-(5'-(4-(DiphenylaMino)phenyl)-[2,2'-bithiophen]-5-yl)cyclohex-2-enone synthesis

1synthesis methods

Product Name:3-(5'-(4-(DiphenylaMino)phenyl)-[2,2'-bithiophen]-5-yl)cyclohex-2-enone
CAS Number:1096156-10-3
Molecular formula:C32H25NOS2
Molecular Weight:503.68

3-(5'-BroMo-[2,2'-bithiophen]-5-yl)cyclohex-2-enone

1096156-08-9
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201802-67-7
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$6.00/1g

3-(5'-(4-(DiphenylaMino)phenyl)-[2,2'-bithiophen]-5-yl)cyclohex-2-enone

1096156-10-3
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Yield:1096156-10-3 80%

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;sodium carbonate in ethanol;water;toluene;Inert atmosphere;Reflux;Suzuki coupling;

References:

Chen, Kuan-Fu;Hsu, Ying-Chan;Wu, Qiongyou;Yen, Ming-Chang P.;Sun, Shih-Sheng [Organic Letters,2009,vol. 11,# 2,p. 377 - 380] Location in patent:supporting information; experimental part