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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

11-Hexadecynal synthesis

2synthesis methods
1-Heptadecen-12-yne

114971-83-4
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11-Hexadecynal

86426-73-5
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Yield:86426-73-5 80%

Reaction Conditions:

Stage #1: heptadec-1-en-12-ynewith oxygen;ozone in methanol;cyclohexane at 5;
Stage #2: with dimethylsulfide in tetrahydrofuran at 5; for 6 h;

References:

Ishmuratov;Botsman;Botsman;Yakovleva;Kharisov;Tolstikov [Chemistry of Natural Compounds,2000,vol. 36,# 2,p. 207 - 209]

11-BROMO-1-UNDECENE

7766-50-9
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$8.00/1g

11-Hexadecynal

86426-73-5
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References