11-Hydroxy-5H-dibenzo[b,e]azepin-6(11H)-one synthesis
- Product Name:11-Hydroxy-5H-dibenzo[b,e]azepin-6(11H)-one
- CAS Number:723-87-5
- Molecular formula:C14H11NO2
- Molecular Weight:225.24
84-65-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: sodium azide; sulfuric acid / chloroform / 12 h / Reflux
2: sodium tetrahydroborate / methanol / 3 h / 0 - 20 °C
References:
Mittapalli, Gopi Kumar;Vellucci, Danielle;Yang, Jun;Toussaint, Marion;Brothers, Shaun P.;Wahlestedt, Claes;Roberts, Edward [Bioorganic and Medicinal Chemistry Letters,2012,vol. 22,# 12,p. 3916 - 3920]
1143-50-6
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