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ChemicalBook CAS DataBase List 11-Hydroxy-sugiol
88664-08-8

11-Hydroxy-sugiol synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 71.4 percent / CHCl3 / 7 h / 20 °C
2: 76.7 percent / TsOH / toluene / 5 h / Heating
3: 65.9 percent / CrO3 / acetic acid / 8 h / 20 °C
4: 96.3 percent / NaHCO3 / methanol; H2O / 1.5 h / Heating

References:

Yang, Zhixiang;Kitano, Yoshikazu;Chiba, Kazuhiro;Shibata, Naohiro;Kurokawa, Hiroshi;Doi, Yohei;Arakawa, Yoshichika;Tada, Masahiro [Bioorganic and Medicinal Chemistry,2001,vol. 9,# 2,p. 347 - 356]

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