11-(iodomethyl)tricosane synthesis
- Product Name:11-(iodomethyl)tricosane
- CAS Number:1143585-16-3
- Molecular formula:C24H49I
- Molecular Weight:464.55
58670-89-6
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Yield:1143585-16-3 73%
Reaction Conditions:
with hydrogen iodide in water;Heating / reflux;
Steps:
19.a
228.06g of 2-decyl-1-tetradecanol [58670-89-6] are mixed with 484.51 g 47% hydroiodic acid and the mixture is refluxed overnight. The product is extracted with t-butyl-methylether. Then the organic phase is dried and concentrated. The product is purified over a silica gel column to give 211.54 g of the desired compound 51 (73%). 1H-NMR (ppm, CDCI3): 3.26 2H d, 1.26-1.12 41 H m, 0.88 6H t.
References:
WO2009/47104,2009,A2 Location in patent:Page/Page column 54
58670-89-6
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10034-85-2
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1143585-16-3
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