11-(METHACRYLOYLAMINO)UNDECANOIC ACID synthesis
- Product Name:11-(METHACRYLOYLAMINO)UNDECANOIC ACID
- CAS Number:59178-93-7
- Molecular formula:C15H27NO3
- Molecular Weight:269.38
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Yield:59178-93-7 92%
Reaction Conditions:
with sodium carbonate in tetrahydrofuran;water at 0; for 5 h;
Steps:
1
Example 1; [0049] Synthesis of 11 -Methacrylamidoundecanoic Acid; 10-Aminodecanoic acid (4.04 g, 20 mmol) was dissolved in 300 ml of THF and water (1 :1 ) in an ice-water bath, and then sodium carbonate (3.18 g, 30 mmol) was added. Methacryloyl chloride (3.15 g, 30 mmol) was slowly added, and the mixture was
References:
WO2008/100907,2008,A2 Location in patent:Page/Page column 26-27