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ChemicalBook CAS DataBase List L-3-methyl-2-(pyridine-4-yl-methylamino)butanoicacid
1105060-26-1

L-3-methyl-2-(pyridine-4-yl-methylamino)butanoicacid synthesis

1synthesis methods
-

Yield:1105060-26-1 70%

Reaction Conditions:

Stage #1: pyridine-4-carbaldehyde;L-valinewith sodium carbonate in methanol;water; for 3 h;Cooling with ice;
Stage #2: with sodium tetrahydroborate in methanol;water; for 12 h;Cooling with ice;

References:

Saha, Subhadeep;Das, Gobinda;Thote, Jayshri;Banerjee, Rahul [Journal of the American Chemical Society,2014,vol. 136,# 42,p. 14845 - 14851] Location in patent:supporting information