2-[2-Hydroxyethyl]-9-[beta-d-ribofuranosyl]hypoxanthine synthesis

3synthesis methods

Product Name:2-[2-Hydroxyethyl]-9-[beta-d-ribofuranosyl]hypoxanthine
CAS Number:110851-59-7
Molecular formula:C12H16N4O6
Molecular Weight:312.28

2',3',5'-Tri-O-acetyl-2-aMino-6-chloropurine Riboside

16321-99-6
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2-[2-Hydroxyethyl]-9-[beta-d-ribofuranosyl]hypoxanthine

110851-59-7
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Yield:-

Steps:

Multi-step reaction with 6 steps
1: n-C₅H₁₁NO, CH₂I₂ / acetonitrile
2: 96 percent / NaOMe
3: 96 percent / imidazole / dimethylformamide
4: 95 percent / PdCl₂(CH₃CN)2 / toluene / Heating
5: 1.) 9-BBN / tetrahydrofuran / Heating
6: 1.) (CH₃)3SiI, 2.) Et₄NF / acetonitrile

References:

Nair;Turner;Chamberlain [Journal of the American Chemical Society,1987,vol. 109,# 23,p. 7223 - 7224]

ACETIC ACID (2R,3R,4R,5R)-3,4-DIACETOXY-5-(6-CHLORO-2-IODO-PURIN-9-YL)-TETRAHYDRO-FURAN-2-YLMETHYL ESTER

5987-76-8
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$61.00/1g

110851-59-7
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References

114763-45-0
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110851-59-7
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References