(E)-3,5-dichloro-4-(3-ethoxy-2-methyl-3-oxoprop-1-enyl)benzoic acid synthesis
- Product Name:(E)-3,5-dichloro-4-(3-ethoxy-2-methyl-3-oxoprop-1-enyl)benzoic acid
- CAS Number:1110767-89-9
- Molecular formula:C13H12Cl2O4
- Molecular Weight:303.14
51-36-5
364 suppliers
$7.00/25g
1110767-89-9
69 suppliers
$23.00/250mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / -50 °C / Inert atmosphere; Industrial scale
1.2: -50 °C / Inert atmosphere; Industrial scale
2.1: lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Industrial scale
2.2: 3.5 h / 0 - 15 °C / Inert atmosphere; Industrial scale
References:
Imamura, Yoshiaki;Kakinuma, Makoto;Komurasaki, Tadafumi;Matsuura, Takaharu;Nishino, Yutaka;Sato, Yusuke [Organic Process Research and Development,2020,vol. 24,# 11,p. 2651 - 2656]
153203-80-6
59 suppliers
$15.00/100mg
3699-66-9
212 suppliers
$8.00/5g
1110767-89-9
69 suppliers
$23.00/250mg