tert-butyl 5-oxo-5,6,7,8-tetrahydronaphthalen-2-ylcarbaMate synthesis

1synthesis methods

Product Name:tert-butyl 5-oxo-5,6,7,8-tetrahydronaphthalen-2-ylcarbaMate
CAS Number:1116358-98-5
Molecular formula:C15H19NO3
Molecular Weight:261.3163

Carbamic acid, N-(5,6,7,8-tetrahydro-2-naphthalenyl)-, 1,1-dimethylethyl ester

1116358-94-1
0 suppliers
inquiry

tert-butyl 5-oxo-5,6,7,8-tetrahydronaphthalen-2-ylcarbaMate

1116358-98-5
7 suppliers
inquiry

Yield:1116358-98-5 65%

Reaction Conditions:

with pyridinium chlorochromate in dichloromethane; for 24 h;Reflux;Molecular sieve;

References:

Lim, Ju-Ok;Jin, Mi-Kyoung;Ryu, HyungChul;Kang, Dong Wook;Lee, Jeewoo;Pearce, Larry V.;Tran, Richard;Toth, Attila;Blumberg, Peter M. [European Journal of Medicinal Chemistry,2009,vol. 44,# 1,p. 322 - 331] Location in patent:experimental part