Ethyl 4-chloro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate synthesis

1synthesis methods

Product Name:Ethyl 4-chloro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate
CAS Number:1146214-96-1
Molecular formula:C15H20BClO4
Molecular Weight:310.5809

7335-27-5
128 suppliers
$10.00/1g

73183-34-3
569 suppliers
$6.00/5g

Ethyl 4-chloro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

1146214-96-1
9 suppliers
inquiry

Yield:1146214-96-1 87%

Reaction Conditions:

with silica-SMAP-Ir(OCH₃)(C₈H₁₂) in hexane;ligand reacted with B-compound in hexane in presence of Ir-complex as catalyst at 70°C for 20 h;

References:

Kawamorita, Soichiro;Ohmiya, Hirohisa;Hara, Kenji;Fukuoka, Atsushi;Sawamura, Masaya [Journal of the American Chemical Society,2009,vol. 131,p. 5058 - 5059]