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1-tert-butyl 2-Methyl 2-(2-oxoethyl)azetidine-1,2-dicarboxylate synthesis

1synthesis methods
1148044-26-1 Synthesis
1-tert-butyl 2-Methyl 2-(3-Methylbut-2-enyl)azetidine-1,2-dicarboxylate

1148044-26-1
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1-tert-butyl 2-Methyl 2-(2-oxoethyl)azetidine-1,2-dicarboxylate

1148044-27-2
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Yield:1148044-27-2 75%

Reaction Conditions:

with ozone;triphenylphosphine in methanol;dichloromethane at -65;

References:

Sippy, Kevin B.;Anderson, David J.;Bunnelle, William H.;Hutchins, Charles W.;Schrimpf, Michael R. [Bioorganic and Medicinal Chemistry Letters,2009,vol. 19,# 6,p. 1682 - 1685] Location in patent:scheme or table