1-(tert-Butoxycarbonyl)pyrrole-2-boronic acid MIDA ester synthesis
- Product Name:1-(tert-Butoxycarbonyl)pyrrole-2-boronic acid MIDA ester
- CAS Number:1158984-94-1
- Molecular formula:C14H19BN2O6
- Molecular Weight:322.1215
5176-27-2
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$10.00/1g
4408-64-4
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$6.00/5g
1158984-94-1
35 suppliers
$55.00/250mg
Yield:1158984-94-1 29%
Reaction Conditions:
Stage #1: N-tert-butyloxycarbonyl-pyrrolewith n-butyllithium;Triisopropyl borate;N-ethyl-N,N-diisopropylamine in tetrahydrofuran;hexane at -78 - 20;
Stage #2: N-methyliminodiacetic acid in dimethyl sulfoxide at 75; under 1 Torr; for 2 h;
References:
Knapp, David M.;Gillis, Eric P.;Burke, Martin D. [Journal of the American Chemical Society,2009,vol. 131,p. 6961 - 6963] Location in patent:supporting information; experimental part
4408-64-4
178 suppliers
$6.00/5g
135884-31-0
310 suppliers
$14.00/1g
1158984-94-1
35 suppliers
$55.00/250mg