ChemicalBook CAS DataBase List (2S)-2-amino-6-{[(2-azidoethoxy)carbonyl]amino}hexanoic acid

(2S)-2-amino-6-{[(2-azidoethoxy)carbonyl]amino}hexanoic acid synthesis

3synthesis methods

Product Name:(2S)-2-amino-6-{[(2-azidoethoxy)carbonyl]amino}hexanoic acid
CAS Number:1167421-25-1
Molecular formula:C9H17N5O4
Molecular Weight:259.27

13734-28-6
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(2S)-2-amino-6-{[(2-azidoethoxy)carbonyl]amino}hexanoic acid

1167421-25-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: sodium hydroxide / water / 18.5 h / 20 °C
2: sodium azide / N,N-dimethyl-formamide / 48 h / 70 °C
3: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

References:

Milles, Sigrid;Tyagi, Swati;Banterle, Niccolo;Koehler, Christine;Vandelinder, Virginia;Plass, Tilman;Neal, Adrian P.;Lemke, Edward A. [Journal of the American Chemical Society,2012,vol. 134,# 11,p. 5187 - 5195]

L-Lysine, N6-[(2-azidoethoxy)carbonyl]-N2-[(1,1-dimethylethoxy)carbonyl]-

1167421-24-0
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1167421-25-1
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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1167421-25-1
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References

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