1-Benzenesulfonyl-3-broMo-1H-pyrrolo[2,3-c]pyridine synthesis
- Product Name:1-Benzenesulfonyl-3-broMo-1H-pyrrolo[2,3-c]pyridine
- CAS Number:1174038-64-2
- Molecular formula:C13H9BrN2O2S
- Molecular Weight:337.19
271-29-4
269 suppliers
$9.00/250mg
1174038-64-2
21 suppliers
$265.00/500 mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: bromine; sodium hydrogencarbonate / methanol / 3 h / 0 - 20 °C / Inert atmosphere
2: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere
References:
Kettle, Jason G.;Ballard, Peter;Bardelle, Catherine;Cockerill, Mark;Colclough, Nicola;Critchlow, Susan E.;Debreczeni, Judit;Fairley, Gary;Fillery, Shaun;Graham, Mark A.;Goodwin, Louise;Guichard, Sylvie;Hudson, Kevin;Ward, Richard A.;Whittaker, David [Journal of Medicinal Chemistry,2015,vol. 58,# 6,p. 2834 - 2844]
98-09-9
341 suppliers
$12.00/25 g
67058-76-8
125 suppliers
$32.00/250 mg
1174038-64-2
21 suppliers
$265.00/500 mg