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1174372-96-3

(4-Chlorophenyl)(3,3-dimethyl-2-(p-tolyloxy)indolin-1-yl)methanone synthesis

1synthesis methods
Methanone, (4-chlorophenyl)(2,3-dihydro-2-hydroxy-3,3-dimethyl-1H-indol-1-yl)-

51459-50-8
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(4-Chlorophenyl)(3,3-dimethyl-2-(p-tolyloxy)indolin-1-yl)methanone

1174372-96-3
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Yield:1174372-96-3 71%

Reaction Conditions:

with boron trifluoride diethyl etherate in diethyl ether at 0; for 2 h;Inert atmosphere;

References:

Eto, Masashi;Ito, Fumikazu;Sato, Hidetoshi;Shinohara, Itaru;Yamaguchi, Koki;Yoshitake, Yasuyuki;Harano, Kazunobu [Heterocycles,2009,vol. 78,# 6,p. 1485 - 1496] Location in patent:experimental part