ChemicalBook CAS DataBase List 8-Chloro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-one

8-Chloro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-one synthesis

1synthesis methods

Product Name:8-Chloro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-one
CAS Number:117811-16-2
Molecular formula:C14H8ClNO
Molecular Weight:241.67

31251-41-9 Synthesis

8-Chloro-5,6-dihydro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-one

31251-41-9
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8-Chloro-11H-benzo[5,6]cyclohepta[1,2-b]pyridin-11-one

117811-16-2
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Yield:-

Reaction Conditions:

with N-Bromosuccinimide;2,2'-azobis(isobutyronitrile);1,8-diazabicyclo[5.4.0]undec-7-ene1) CCl₄, reflux, 1.25 h; 2) CH₂Cl₂, reflux, 1 h;Yield given. Multistep reaction;

References:

Piwinski, John J.;Wong, Jesse K.;Chan, Tze-Ming;Green, Michael J.;Ganguly, Ashit K. [Journal of Organic Chemistry,1990,vol. 55,# 10,p. 3341 - 3350]