4-METHOXY-3-(2,2,2-TRIFLUOROACETAMIDO)BENZENESULFONYL CHLORIDE synthesis

2synthesis methods

Product Name:4-METHOXY-3-(2,2,2-TRIFLUOROACETAMIDO)BENZENESULFONYL CHLORIDE
CAS Number:1184086-20-1
Molecular formula:C9H7ClF3NO4S
Molecular Weight:317.67

AcetaMide, 2,2,2-trifluoro-N-(2-Methoxyphenyl)-

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4-METHOXY-3-(2,2,2-TRIFLUOROACETAMIDO)BENZENESULFONYL CHLORIDE

1184086-20-1
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Yield:1184086-20-1 77%

Reaction Conditions:

with chlorosulfonic acid in dichloromethane at 0 - 20; for 16 h;Inert atmosphere;

References:

Whitehouse, Andrew J.;Libardo, M. Daben J.;Kasbekar, Monica;Brear, Paul D.;Fischer, Gerhard;Thomas, Craig J.;Barry, Clifton E.;Boshoff, Helena I. M.;Coyne, Anthony G.;Abell, Chris [Journal of Medicinal Chemistry,2019,vol. 62,# 23,p. 10586 - 10604] Location in patent:supporting information

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1184086-20-1
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References