ChemicalBook CAS DataBase List D-Glucitol, 1,5-anhydro-1-C-[4-chloro-3-(phenylmethyl)phenyl]-, (1S)-

D-Glucitol, 1,5-anhydro-1-C-[4-chloro-3-(phenylmethyl)phenyl]-, (1S)- synthesis

4synthesis methods

Product Name:D-Glucitol, 1,5-anhydro-1-C-[4-chloro-3-(phenylmethyl)phenyl]-, (1S)-
CAS Number:1185339-44-9
Molecular formula:C19H21ClO5
Molecular Weight:364.82

312749-31-8
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D-Glucitol, 1,5-anhydro-1-C-[4-chloro-3-(phenylmethyl)phenyl]-, (1S)-

1185339-44-9
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux
2: n-butyllithium / tetrahydrofuran; toluene / -78 °C
3: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C
4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C

References:

Xu, Baihua;Feng, Yan;Cheng, Huawei;Song, Yanli;Lv, Binhua;Wu, Yuelin;Wang, Congna;Li, Shengbin;Xu, Min;Du, Jiyan;Peng, Kun;Dong, Jiajia;Zhang, Wenbin;Zhang, Ting;Zhu, Liangcheng;Ding, Haifeng;Sheng, Zelin;Welihinda, Ajith;Roberge, Jacques Y.;Seed, Brian;Chen, Yuanwei [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 15,p. 4465 - 4470]

Benzene, 4-bromo-1-chloro-2-(phenylmethyl)-

1185339-38-1
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References

21739-92-4 Synthesis

21739-92-4
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$8.00/10g

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References

71-43-2
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$11.19/25ML

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References