1-[1-(4-fluorophenyl)ethyl]-3-hydroxypiperidin-2-one synthesis
- Product Name:1-[1-(4-fluorophenyl)ethyl]-3-hydroxypiperidin-2-one
- CAS Number:1186046-94-5
- Molecular formula:C13H16FNO2
- Molecular Weight:237.27
403-40-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: pyridine / dichloromethane / Cooling with ice
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 60 °C
3.1: tert.-butyl lithium / tetrahydrofuran / 0.25 h / -78 °C
3.2: 0.33 h / -78 °C
References:
WO2009/108766,2009,A1
1119-46-6
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19347-73-0
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$232.00/1g
1186046-94-5
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