ChemicalBook CAS DataBase List TERT-BUTYL5-FLUORO-2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYLCARBAMATE

TERT-BUTYL5-FLUORO-2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYLCARBAMATE synthesis

4synthesis methods

Product Name:TERT-BUTYL5-FLUORO-2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYLCARBAMATE
CAS Number:1186637-38-6
Molecular formula:C17H25BFNO4
Molecular Weight:337.19

24424-99-5 Synthesis

24424-99-5
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TERT-BUTYL5-FLUORO-2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PHENYLCARBAMATE

1186637-38-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C / Inert atmosphere
1.2: 0 - 20 °C
2.1: sodium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C / Inert atmosphere

References:

IRM LLC;NOVARTIS AG. WO2009/111337, 2009, A1

861931-75-1 Synthesis