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2-Propen-1-one, 3-(dimethylamino)-1-(4-pyrimidinyl)- synthesis

1synthesis methods
4637-24-5 Synthesis
N,N-Dimethylformamide dimethyl acetal

4637-24-5
593 suppliers
$5.00/25g

39870-05-8 Synthesis
Ethanone,1-(4-pyrimidinyl)-

39870-05-8
107 suppliers
$67.00/100mg

2-Propen-1-one, 3-(dimethylamino)-1-(4-pyrimidinyl)-

1190280-82-0
1 suppliers
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Yield:1190280-82-0 87%

Reaction Conditions:

in N,N-dimethyl-formamide at 150; for 18 h;

References:

Curtis, Michael P.;Sammons, Matthew F.;Piotrowski, David W. [Tetrahedron Letters,2009,vol. 50,# 39,p. 5479 - 5481] Location in patent:scheme or table