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(2-Amino-ethyl)-isopropyl-carbamic acid tert-butyl ester synthesis

3synthesis methods
Carbamic acid, N-[2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)ethyl]-N-(1-methylethyl)-, 1,1-dimethylethyl ester

1198081-73-0
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(2-Amino-ethyl)-isopropyl-carbamic acid tert-butyl ester

1190889-97-4
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Yield:1190889-97-4 83%

Reaction Conditions:

with hydrazine hydrate in methanol at 60; for 4.5 h;Reflux;

References:

Li, Hongbo;Hao, Meng-An;Wang, Liping;Liang, Wu;Chen, Kai [Organic Preparations and Procedures International,2009,vol. 41,# 4,p. 301 - 307] Location in patent:experimental part

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