2-OXO-2,3-DIHYDRO-1H-BENZO[D]IMIDAZOL-5-YLBORONIC ACID synthesis

3synthesis methods

Product Name:2-OXO-2,3-DIHYDRO-1H-BENZO[D]IMIDAZOL-5-YLBORONIC ACID
CAS Number:1194483-04-9
Molecular formula:C7H7BN2O3
Molecular Weight:177.95

710348-69-9 Synthesis

2-Oxo-2,3-dihydro-1H-benzoimidazole-5-boronic acid, pinacol ester

710348-69-9
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2-OXO-2,3-DIHYDRO-1H-BENZO[D]IMIDAZOL-5-YLBORONIC ACID

1194483-04-9
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Yield:1194483-04-9 7.4%

Reaction Conditions:

with sodium periodate;ammonium acetate in water;acetone at 45 - 55; for 5 h;Inert atmosphere;

References:

Adamson, Christopher;Kajino, Hidetoshi;Kanai, Motomu;Kawashima, Shigehiro A.;Yamatsugu, Kenzo [Journal of the American Chemical Society,2021,vol. 143,# 37,p. 14976 - 14980] Location in patent:supporting information