Methyl 3-bromo-5-ethoxy-6-oxo-1,6-dihydropyridine-2-carboxylate synthesis

1synthesis methods

Product Name:Methyl 3-bromo-5-ethoxy-6-oxo-1,6-dihydropyridine-2-carboxylate
CAS Number:1196959-77-9
Molecular formula:C9H10BrNO4
Molecular Weight:276.08

2-Pyridinecarboxylic acid, 5-ethoxy-1,6-dihydro-6-oxo-, methyl ester

1196959-36-0
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Methyl 3-bromo-5-ethoxy-6-oxo-1,6-dihydropyridine-2-carboxylate

1196959-77-9
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Yield:1196959-77-9 74%

Reaction Conditions:

with N-Bromosuccinimide in dichloromethane;Reflux;

References:

Donohoe, Timothy J.;Bower, John F.;Basutto, José A.;Fishlock, Lisa P.;Procopiou, Panayiotis A.;Callens, Cedric K.A. [Tetrahedron,2009,vol. 65,# 44,p. 8969 - 8980] Location in patent:experimental part