ChemicalBook CAS DataBase List tert-butyl 4-(benzo[d]isoxazol-3-yl)piperidine-1-carboxylate

tert-butyl 4-(benzo[d]isoxazol-3-yl)piperidine-1-carboxylate synthesis

1synthesis methods

Product Name:tert-butyl 4-(benzo[d]isoxazol-3-yl)piperidine-1-carboxylate
CAS Number:1198283-78-1
Molecular formula:C17H22N2O3
Molecular Weight:302.37

88284-48-4 Synthesis

2-(TRIMETHYLSILYL)PHENYL TRIFLUOROMETHANESULFONATE

88284-48-4
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1-Piperidinecarboxylic acid, 4-[chloro(hydroxyimino)methyl]-, 1,1-dimethylethyl ester

467423-44-5
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tert-butyl 4-(benzo[d]isoxazol-3-yl)piperidine-1-carboxylate

1198283-78-1
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Yield:1198283-78-1 88%

Reaction Conditions:

with cesium fluoride in dichloromethane;acetonitrile at 20; for 6 h;

References:

Dubrovskiy, Anton V.;Jain, Prashi;Shi, Feng;Lushington, Gerald H.;Santini, Conrad;Porubsky, Patrick;Larock, Richard C. [ACS Combinatorial Science,2013,vol. 15,# 4,p. 193 - 201] Location in patent:supporting information