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ChemicalBook CAS DataBase List 12-Azidododecylphosphonic acid, 95%
721457-32-5

12-Azidododecylphosphonic acid, 95% synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 4 h / 160 °C
2.1: sodium azide / ethanol / 40 h / Reflux
3.1: trimethylsilyl bromide / dichloromethane / 20 °C / Inert atmosphere
3.2: 2 h / Inert atmosphere

References:

Toulemon, Delphine;Pichon, Benoiit P.;Leuvrey, Cedric;Zafeiratos, Spyridon;Papaefthimiou, Vasiliki;Cattoen, Xavier;Begin-Colin, Sylvie [Chemistry of Materials,2013,vol. 25,# 14,p. 2849 - 2854]