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ChemicalBook CAS DataBase List Methyl 5-acetamido-4,7,8,9-tetra-O-benzyl-2-chloro-2,3,5-trideoxy-3-phenylthio-D-erytho-L-gluco-2-nonulopyranosonate

Methyl 5-acetamido-4,7,8,9-tetra-O-benzyl-2-chloro-2,3,5-trideoxy-3-phenylthio-D-erytho-L-gluco-2-nonulopyranosonate synthesis

2synthesis methods
D-erythro-L-gluco-2-Nonulopyranosonic acid, 5-(acetylamino)-5-deoxy-3-S-phenyl-4,7,8,9-tetrakis-O-(phenylmethyl)-3-thio-, methyl ester

139684-71-2
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Methyl 5-acetamido-4,7,8,9-tetra-O-benzyl-2-chloro-2,3,5-trideoxy-3-phenylthio-D-erytho-L-gluco-2-nonulopyranosonate

120308-52-3
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Yield:120308-52-3 99%

Reaction Conditions:

with tetrachloromethane;Hexamethylphosphorous triamide in tetrahydrofuran;from -78 deg C to 20 deg C;

References:

Ito, Yukishige;Ogawa, Tomoya [Tetrahedron Letters,1988,vol. 29,# 32,p. 3987 - 3990]